N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide
• CAS No.: 1029801-43-1
• Molecular Formula: C₂₃H₂₇NO₄S
• Molecular Weight: 413.538

Synonyms:N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide

Chemical Property of N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide

There total 1 articles about N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide (1029801-33-9) + allyl bromide (106-95-6) → N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide (1029801-43-1)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; toluene; at 20 ℃; for 0.5h;

DOI:10.1021/ja802906k

Reference yield: 87.0%

N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide (1029801-43-1) → (1S*,4S*,7S*)-4-(3,5-dimethoxyphenyl)-5-methylene-3-tosyl-3-azabicyclo[5.1.0]octane

Guidance literature:

With 1,2-bis-(diphenylphosphino)ethane; di(rhodium)tetracarbonyl dichloride; In toluene; at 110 ℃; for 0.5h;

DOI:10.1021/ja802906k

Reference yield: 67.0%

N-allyl-N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide (1029801-43-1) → (1S*,2R*,5R*)-1-allyl-2-(3,5-dimethoxyphenyl)-3-tosyl-3-azabicyclo[3.1.0]hexane

Guidance literature:

With triphenylphosphine; [Rh(CH₂=CH₂)2Cl]2; In toluene; at 110 ℃; for 0.166667h;

DOI:10.1021/ja802906k

upstream raw materials:

N-(bicyclo[1.1.0]but-1-yl(3,5-dimethoxyphenyl)methyl)-4-methylbenzenesulfonamide

allyl bromide

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