(R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

Base Information

Chemical Name:(R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther
CAS No.:153441-19-1
Molecular Formula:C₂₀H₂₀FNO₂S
Molecular Weight:357.449
Hs Code.:

Synonyms:(R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

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Chemical Property of (R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

Chemical Property:

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Technology Process of (R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

There total 4 articles about (R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[(R)-1-(3-Benzyloxy-5-fluoro-phenyl)-1-methoxy-propyl]-2,5-dihydro-thiazole

: 153441-19-1
(R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 3h; Yield given; Heating;
DOI:10.1021/jm00027a014

Reference yield:

: 153441-17-9
(R)-(+)-2-<3-(benzyloxy)-5-fluorophenyl>-2-methoxybutanal

: 153441-19-1
(R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂SO₄, NH₃(gas) / tetrahydrofuran / Heating

2: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 3 h / Heating

With ammonia; sodium sulfate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; benzene;
DOI:10.1021/jm00027a014

Reference yield:

: 153441-15-7
(R)-(-)-2-<3-(benzyloxy)-5-fluorophenyl>-2-methoxybutanol

: 153441-19-1
(R)-(-)-1-<3-(benzyloxy)-5-fluorophenyl>-1-(thiazol-2-yl)propyl methyl 4ther

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / DMSO, oxalyl chloride / CH₂Cl₂ / 1.25 h / -60 - 20 °C

2: Na₂SO₄, NH₃(gas) / tetrahydrofuran / Heating

3: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 3 h / Heating

With oxalyl dichloride; ammonia; dimethyl sulfoxide; sodium sulfate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jm00027a014