Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

Base Information

Chemical Name:Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester
CAS No.:186410-31-1
Molecular Formula:C₂₂H₂₇NO₄Se
Molecular Weight:448.421
Hs Code.:

Synonyms:Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

Suppliers and Price of Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

There total 3 articles about Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 186410-31-1
Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 4-Angstroem molecular sieves / diethyl ether / 1 h / 0 °C

2: 2.) DIBALH / 1.) Et₂O, r.t., 2.) toluene, Et₂O, r.t., 3 h

With 4 A molecular sieve; diisobutylaluminium hydride; In diethyl ether;
DOI:10.1002/hlca.19980810216

Reference yield:

: 1666-13-3
diphenyl diselenide

: 541-41-3
chloroformic acid ethyl ester

: 131319-74-9
(R)-2,3-di-O-isoproylideneglyceraldehyde N-benzylimine

: 186410-31-1
Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

Guidance literature:: With diisobutylaluminium hydride; Yield given. Multistep reaction; 1.) Et₂O, r.t., 2.) toluene, Et₂O, r.t., 3 h;
DOI:10.1002/hlca.19980810216

Reference yield:

: 541-41-3
chloroformic acid ethyl ester

: 131319-74-9
(R)-2,3-di-O-isoproylideneglyceraldehyde N-benzylimine

: 85028-55-3
phenylselanyldiisobutylaluminum

: 186410-31-1
Benzyl-[((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenylselanyl-methyl]-carbamic acid ethyl ester

Guidance literature:: Yield given. Multistep reaction; 1.) Et₂O, 0 deg C to room temp., 2.) Et₂O, toluene, -10 deg C, 1 h;
DOI:10.1016/S0040-4039(96)02160-0