2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl-
CAS No.:79759-59-4
Molecular Formula:C19H13ClN2O
Molecular Weight:320.778
Hs Code.:
DSSTox Substance ID:DTXSID10229881
Wikidata:Q83110252

Synonyms:BRN 5587163;1,3-Diphenyl-5-chloro-benzimidazolin-2-one;2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl-;79759-59-4;1,3-Dihydro-5-chloro-1,3-diphenyl-2H-benzimidazol-2-one;C19H13ClN2O;C19-H13-Cl-N2-O;DTXSID10229881;LS-33307

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl-

Chemical Property:

Vapor Pressure:1.52E-09mmHg at 25°C
Boiling Point:484.6°C at 760 mmHg
Flash Point:246.9°C
Density:1.35g/cm³
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:320.0716407
Heavy Atom Count:23
Complexity:431

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C3=C(C=C(C=C3)Cl)N(C2=O)C4=CC=CC=C4

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl-

There total 3 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1,3-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.31%

: 32315-10-9
bis(trichloromethyl) carbonate

: C₁₈H₁₅ClN₂

: 79759-59-4
1,3-diphenyl-5-chloro-benzimidazolin-2-one

Guidance literature:: bis(trichloromethyl) carbonate; C₁₈H₁₅ClN₂; With triethylamine; In dichloromethane; at -5 - 20 ℃; for 16h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; for 0.5h; Inert atmosphere;

Reference yield: 53.0%

: 26440-44-8
1,5-diphenyl-7-chloro-1,2,4,5-tetrahydro-2,4-dioxo-3H-1,5-benzodiazephine

: 79759-59-4
1,3-diphenyl-5-chloro-benzimidazolin-2-one

Guidance literature:: With sodium ethanolate; In ethanol; for 18h; Ambient temperature;

Reference yield:

: 89-63-4
4-Chloro-2-nitroaniline

: 79759-59-4
1,3-diphenyl-5-chloro-benzimidazolin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; palladium diacetate / toluene / 4 h / 105 - 110 °C / Inert atmosphere

2.1: 2 h / -15 - -10 °C / Inert atmosphere

2.2: 3 h / 20 - 25 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 16 h / -5 - 20 °C / Inert atmosphere

3.2: 0.5 h / Inert atmosphere

With palladium diacetate; triethylamine; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In dichloromethane; toluene;