(η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

Base Information

Chemical Name:(η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)
CAS No.:856702-73-3
Molecular Formula:C₂₆H₂₂CrN₃O₂PS
Molecular Weight:523.515
Hs Code.:

Synonyms:(η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

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Chemical Property of (η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

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Technology Process of (η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

There total 1 articles about (η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 856702-66-4
(2-phenylthiopyrrolyl)dipyrrolylphosphine

: 697302-50-4,697302-51-5,12082-08-5,697302-53-7
(benzene)tricarbonylchromium

: 856702-73-3
(η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

Guidance literature:: With cis-Cyclooctene; In benzene; Irradiation (UV/VIS); (Ar), Cr complex slowly treated with benzene and cyclooctene, irradiatedfor 1 h (Hg lamp), slowly treated with ligand in benzene, stirred for 3 0 min; filtered (celite), evapd.(vac.), chromy.(silica gel hexanes/EtOAc 20:1, evapd.(vac.);
DOI:10.1021/ja042705x

Reference yield:

: 856702-73-3
(η6-benzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

: 1076-43-3
benzene-d6

: (η6-perdeuteriobenzene)(2-(phenylthiopyrrolyl)dipyrrolylphosphine)dicarbonyl chromium(0)

Guidance literature:: In neat (no solvent); byproducts: benzene; in NMR tube; mixed, sealed, preheated to 40-70°C; not isolated, detected by NMR; Kinetics;
DOI:10.1021/ja042705x