2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

Base Information

Chemical Name:2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine
CAS No.:102562-13-0
Molecular Formula:C₄₀H₃₉N₇O₁₆
Molecular Weight:873.787
Hs Code.:

Synonyms:2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

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Chemical Property of 2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

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Technology Process of 2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

There total 9 articles about 2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 20264-96-4
2-(4-nitrophenyl)ethyl iodide

: 102562-12-9
2',3',5'-tri-O-acetyl-2,6-bis<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-7H-purin-8(9H)-one

: 102562-13-0
2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

Guidance literature:: silver (I) ion;
DOI:10.1016/S0040-4039(00)98224-8

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 102562-13-0
2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / triphenylphosphane, diethyl azodicarboxylate / dioxane / 1 h / Ambient temperature

2: 93 percent / NaNO₂, HClO₄ / acetone; H₂O / 1 h / 10 °C

3: 90 percent / Ag₂CO₃ / 1 h / Heating

4: 92 percent / NaOAc / tetradeuterioacetic acid / 3 h / Heating

5: 88 percent / Ag₂CO₃ / CHCl₃; toluene / 6 h / Heating

With perchloric acid; sodium acetate; triphenylphosphine; sodium nitrite; diethylazodicarboxylate; silver carbonate; In 1,4-dioxane; chloroform; water; acetone; toluene;
DOI:10.1002/hlca.19870700126

Reference yield:

: 102604-04-6
2',3',5'-tri-O-acetyl-8-bromo-O⁶-<2-(p-nitrophenyl)ethyl>xanthosine

: 102562-13-0
2',3',5'-tri-O-acetyl-2,6,8-tris<2-(p-nitrophenyl)ethoxy>-9-(β-D-ribofuranosyl)-9H-purine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Ag₂CO₃ / 1 h / Heating

2: 92 percent / NaOAc / tetradeuterioacetic acid / 3 h / Heating

3: 88 percent / Ag₂CO₃ / CHCl₃; toluene / 6 h / Heating

With sodium acetate; silver carbonate; In chloroform; toluene;
DOI:10.1002/hlca.19870700126