5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

Base Information

Chemical Name:5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione
CAS No.:300665-11-6
Molecular Formula:C₂₁H₁₂ClNO₂
Molecular Weight:345.785
Hs Code.:
Nikkaji Number:J2.990.632G

Synonyms:4H-Pyrido[3,2,1-jk]carbazole-4,6(5H)-dione, 5-chloro-5-phenyl-;300665-11-6;5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione;5-Chloro-5-phenyl-4,5-dihydro-6H-pyrido[3,2,1-jk]carbazole-4,6-dione

Suppliers and Price of 5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

Chemical Property:

Vapor Pressure:1.34E-11mmHg at 25°C
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:345.0556563
Heavy Atom Count:25
Complexity:586

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2(C(=O)C3=CC=CC4=C3N(C2=O)C5=CC=CC=C45)Cl

Technology Process of 5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

There total 3 articles about 5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 91622-74-1
4-hydroxy-5-phenyl-6H-pyrido[3,2,1-jk]-carbazol-6-one

: 300665-11-6
5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

Guidance literature:: With sulfuryl dichloride; In 1,4-dioxane; at 50 - 90 ℃; regioselective reaction;
DOI:10.1002/jhet.600

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 300665-11-6
5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: Heating

2: sulfuryl dichloride / 1,4-dioxane / 50 - 90 °C

With sulfuryl dichloride; In 1,4-dioxane;
DOI:10.1002/jhet.600

Reference yield:

: 83-13-6
diethyl 2-phenylmalonate

: 300665-11-6
5-chloro-5-phenyl-4H-pyrido[3,2,1-jk]carbazole-4,6(5H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: Heating

2: sulfuryl dichloride / 1,4-dioxane / 50 - 90 °C

With sulfuryl dichloride; In 1,4-dioxane;
DOI:10.1002/jhet.600