1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol

Base Information

• Chemical Name: 1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol
• CAS No.: 1092981-98-0
• Molecular Formula: C₁₅H₁₈O₅S
• Molecular Weight: 310.371

Synonyms:1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol

Chemical Property of 1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol

Chemical Property:

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Technology Process of 1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol

There total 1 articles about 1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-deoxy-2,3:4,6-di-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-β-D-galactopyranoside (1092981-97-9) → 1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol (1092981-98-0)

Guidance literature:

With n-butyllithium; diisopropylamine; In tetrahydrofuran; pentane; at -30 ℃; for 0.25h;

1-deoxy-2,3:4,6-di-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-β-D-galactopyranoside; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h;

DOI:10.1055/s-2008-1067226

Reference yield: 79.0%

1,5-anhydro-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol (1092981-98-0) + tert-butyldimethylsilyl chloride (18162-48-6) → 1,5-anhydro-3-O-tert-butyldimethylsilyl-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol (1092981-81-1)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1055/s-2008-1067226

upstream raw materials:

1-deoxy-2,3:4,6-di-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-β-D-galactopyranoside

Downstream raw materials:

1,5-anhydro-3-O-tert-butyldimethylsilyl-4,6-O-isopropylidene-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol

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