2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

Base Information

Chemical Name:2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline
CAS No.:149180-55-2
Molecular Formula:C₂₁H₂₆N₄S
Molecular Weight:366.53
Hs Code.:

Synonyms:2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

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Chemical Property of 2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

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Technology Process of 2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

There total 4 articles about 2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 149155-81-7
3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

: 149180-55-2
2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 5h; under 760 Torr;
DOI:10.1021/jm00063a013

Reference yield:

: 826-83-5
4(5)-phenyl-5(4)-methylimidazole

: 149180-55-2
2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 50 deg C, 1 h, 2.) DMF, 60 deg C, 3 h

2: 7 N aq. HCl / tetrahydrofuran / 1 h / Ambient temperature

3: 63 percent / EtONa / ethanol / 2 h / Heating

4: 30 percent / H₂ / 10percent Pd/C / ethyl acetate / 5 h / 760 Torr

With hydrogenchloride; hydrogen; sodium ethanolate; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;
DOI:10.1021/jm00063a013

Reference yield:

: 149155-88-4
3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propionaldehyde

: 149180-55-2
2-(dimethylamino)-6-<<3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propyl>thio>aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / EtONa / ethanol / 2 h / Heating

2: 30 percent / H₂ / 10percent Pd/C / ethyl acetate / 5 h / 760 Torr

With hydrogen; sodium ethanolate; palladium on activated charcoal; In ethanol; ethyl acetate;
DOI:10.1021/jm00063a013