Technology Process of C22H28O3
There total 6 articles about C22H28O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate;
In
tetrahydrofuran;
at 120 ℃;
for 7.5h;
diastereoselective reaction;
Inert atmosphere;
Microwave irradiation;
DOI:10.1002/anie.201101842
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C / Inert atmosphere
2: bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate / tetrahydrofuran / 7.5 h / 120 °C / Inert atmosphere; Microwave irradiation
With
bis(tri-t-butylphosphine)palladium(0); tetrabutyl ammonium fluoride; sodium t-butanolate;
In
tetrahydrofuran;
DOI:10.1002/anie.201101842
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: oxygen; copper(II) acetate monohydrate; palladium dichloride / N,N-dimethyl acetamide; water / 25 h / 23 °C / 760.05 Torr
2.1: potassium hydroxide / xylenes / 11 h / 110 °C / Inert atmosphere
3.1: acetonitrile / 22.5 h / Inert atmosphere; UV-irradiation
3.2: 0.5 h / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C / Inert atmosphere
5.1: bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate / tetrahydrofuran / 7.5 h / 120 °C / Inert atmosphere; Microwave irradiation
With
bis(tri-t-butylphosphine)palladium(0); tetrabutyl ammonium fluoride; oxygen; copper(II) acetate monohydrate; potassium hydroxide; palladium dichloride; sodium t-butanolate;
In
tetrahydrofuran; N,N-dimethyl acetamide; water; acetonitrile; xylenes;
DOI:10.1002/anie.201101842
