9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

Base Information

Chemical Name:9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one
CAS No.:500904-77-8
Molecular Formula:C₂₁H₁₆N₆O₃
Molecular Weight:400.396
Hs Code.:

Synonyms:9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

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Chemical Property of 9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

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Technology Process of 9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

There total 3 articles about 9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 98-88-4
benzoyl chloride

: 500904-71-2
9-methoxy-3,4-diaminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

: 500904-77-8
9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

Guidance literature:: With sodium acetate; In 1,4-dioxane; acetic acid; at 20 ℃; for 4h;
DOI:10.1002/1521-4184(200205)335:5<207::AID-ARDP207>3.0.CO;2-5

Reference yield:

: 129797-61-1
3-amino-7-methoxy-1H-pyrazolo[3,4-b]quinoline

: 500904-77-8
9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium ethoxide / 3 h / Heating

1.2: 70 percent / aq. HCl / pH 6

2.1: 80 percent / 30 percent aq. NH₄OH; aq. Na₂S₂O₄ / 0.5 h / 70 - 80 °C

3.1: 60 percent / aq. AcONa / acetic acid; dioxane / 4 h / 20 °C

With ammonium hydroxide; sodium dithionite; sodium ethanolate; sodium acetate; In 1,4-dioxane; acetic acid;
DOI:10.1002/1521-4184(200205)335:5<207::AID-ARDP207>3.0.CO;2-5

Reference yield:

: 500904-68-7
4-amino-9-methoxy-3-nitrosoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

: 500904-77-8
9-methoxy-3-benzoylamino-4-aminoquinolino[2',3'-5,4](3-1H-pyrazolino)[2,3-a]pyrimidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 30 percent aq. NH₄OH; aq. Na₂S₂O₄ / 0.5 h / 70 - 80 °C

2: 60 percent / aq. AcONa / acetic acid; dioxane / 4 h / 20 °C

With ammonium hydroxide; sodium dithionite; sodium acetate; In 1,4-dioxane; acetic acid;
DOI:10.1002/1521-4184(200205)335:5<207::AID-ARDP207>3.0.CO;2-5