N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

Base Information

Chemical Name:N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid
CAS No.:1429875-09-1
Molecular Formula:C₄₀H₃₈ClN₃O₄
Molecular Weight:660.212
Hs Code.:

Synonyms:N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

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Chemical Property of N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

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Technology Process of N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

There total 8 articles about N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.44%

: 85-44-9
phthalic anhydride

: 1429879-06-0
2-(3-{3-[(E)-2-(7-chloroquinolin-2yl)vinyl]phenyl}-3-methylaminopropyl)-N,N-diethylbenzamide

: 1429875-09-1
N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

Guidance literature:: In dichloromethane; at 20 ℃;

Reference yield:

: 1429879-03-7
[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-(2-diethylcarbamoylphenyl)propyl]carbamic acid tert-butyl ester

: 1429875-09-1
N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / 60 °C

2: sulfuric acid / dichloromethane / 1 h

3: dichloromethane / 20 °C

With sulfuric acid; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1429879-05-9
[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-(2-diethylcarbamoylphenyl)propyl]methylcarbamic acid tert-butyl ester

: 1429875-09-1
N-[1-{3-[(E)-2-(7-chloroquinolin-2-yl)vinyl]phenyl}-3-[(2-diethylcarbamoyl)phenyl]propyl]-N-methylphthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / dichloromethane / 1 h

2: dichloromethane / 20 °C

With sulfuric acid; In dichloromethane;