Technology Process of 12-nitro-6,7-dihydro-5H-7a,8-diaza-dibenzo[a,e]azulene
There total 1 articles about 12-nitro-6,7-dihydro-5H-7a,8-diaza-dibenzo[a,e]azulene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C
1.2: 0 - 20 °C
2.1: copper diacetate; palladium diacetate; potassium carbonate / 2,4-dichlorophenoxyacetic acid dimethylamine / 16 h / 90 °C / Inert atmosphere; Sealed tube
With
copper diacetate; palladium diacetate; sodium hydride; potassium carbonate;
In
2,4-dichlorophenoxyacetic acid dimethylamine; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja1090854
