2--4-methoxyacetophenone

Base Information

Chemical Name:2--4-methoxyacetophenone
CAS No.:128739-13-9
Molecular Formula:C₁₇H₁₈N₂O₄
Molecular Weight:314.341
Hs Code.:

2-<N-methyl-N-(2-nitrobenzyl)amino>-4-methoxyacetophenone

Synonyms:2--4-methoxyacetophenone

Suppliers and Price of 2--4-methoxyacetophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--4-methoxyacetophenone

Chemical Property:

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Technology Process of 2--4-methoxyacetophenone

There total 3 articles about 2--4-methoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: 56222-08-3
(2-nitrobenzyl)methylamine

: 89691-67-8
1-(2-bromo-4-methoxyphenyl)ethanone

: 128739-13-9
2--4-methoxyacetophenone

Guidance literature:: With triethylamine; In diethyl ether; for 6h; Ambient temperature;

Reference yield:

: 88-72-2
1-methyl-2-nitrobenzene

: 128739-13-9
2--4-methoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-bromosuccinimide, dibenzoyl peroxide / 1.) carbon tetrachloride, reflux, 4 h., 2.) ethanol, water, room temp., 4 days

2: 87.5 percent / triethylamine / diethyl ether / 6 h / Ambient temperature

With N-Bromosuccinimide; triethylamine; dibenzoyl peroxide; In diethyl ether;

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 128739-13-9
2--4-methoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 45.4 percent / bromine / CHCl₃ / 1 h / 0 - 5 °C

2: 87.5 percent / triethylamine / diethyl ether / 6 h / Ambient temperature

With bromine; triethylamine; In diethyl ether; chloroform;