Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Base Information

Chemical Name:Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester
CAS No.:197845-74-2
Molecular Formula:C₁₇H₃₀O₆
Molecular Weight:330.422
Hs Code.:

Synonyms:Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

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Chemical Property of Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

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Technology Process of Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

There total 4 articles about Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 107-30-2
chloromethyl methyl ether

: 197845-73-1
Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

: 197845-74-2
Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1016/S0040-4039(97)01793-0

Reference yield:

: 74963-00-1
(E)-(2S,3S)-8-acetoxy-2,3-epoxy-2,6-dimethyloct-6-en-1-ol

: 197845-74-2
Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Swern oxidn.

2: Wittig methylenation

3: 40 percent / BF₃*OEt₂ / CH₂Cl₂ / -60 - -15 °C

4: 92 percent / i-Pr₂NEt / CH₂Cl₂ / 12 h / Ambient temperature

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(97)01793-0

Reference yield:

: 197845-72-0
Acetic acid (E)-3-methyl-5-((2S,3S)-3-methyl-3-vinyl-oxiranyl)-pent-2-enyl ester

: 197845-74-2
Acetic acid (1R,2S,3S,6S)-3,6-bis-methoxymethoxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / BF₃*OEt₂ / CH₂Cl₂ / -60 - -15 °C

2: 92 percent / i-Pr₂NEt / CH₂Cl₂ / 12 h / Ambient temperature

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(97)01793-0