Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Base Information

Chemical Name:Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester
CAS No.:197845-73-1
Molecular Formula:C₁₃H₂₂O₄
Molecular Weight:242.315
Hs Code.:

Synonyms:Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

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Technology Process of Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

There total 3 articles about Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 197845-72-0
Acetic acid (E)-3-methyl-5-((2S,3S)-3-methyl-3-vinyl-oxiranyl)-pent-2-enyl ester

: 197845-73-1
Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -60 - -15 ℃;
DOI:10.1016/S0040-4039(97)01793-0

Reference yield:

: 74963-00-1
(E)-(2S,3S)-8-acetoxy-2,3-epoxy-2,6-dimethyloct-6-en-1-ol

: 197845-73-1
Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Swern oxidn.

2: Wittig methylenation

3: 40 percent / BF₃*OEt₂ / CH₂Cl₂ / -60 - -15 °C

With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(97)01793-0

Reference yield:

: Acetic acid (E)-5-((2S,3R)-3-formyl-3-methyl-oxiranyl)-3-methyl-pent-2-enyl ester

: 197845-73-1
Acetic acid (1R,2S,3S,6S)-3,6-dihydroxy-2,6-dimethyl-2-vinyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Wittig methylenation

2: 40 percent / BF₃*OEt₂ / CH₂Cl₂ / -60 - -15 °C

With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(97)01793-0