3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

Base Information

Chemical Name:3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol
CAS No.:133786-59-1
Molecular Formula:C₂₂H₂₂O₄S₂
Molecular Weight:414.546
Hs Code.:

Synonyms:3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

Suppliers and Price of 3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

Chemical Property:

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Technology Process of 3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

There total 2 articles about 3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 133786-57-9
2,6-bis(2-hydroxy-5-methylphenylthio)-4-methylphenol

: 133786-59-1
3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

Guidance literature:: With sodium hydroxide; In methanol; water; at 50 ℃; for 80h;
DOI:10.1246/bcsj.64.576

Reference yield:

: 106-44-5
p-cresol

: 133786-59-1
3-<3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylphenylthio>-2-hydroxy-5-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 4 percent / SCl₂ / CH₂Cl₂

2: 30 percent / 10percent NaOH / methanol; H₂O / 80 h / 50 °C

With sodium hydroxide; sulfur dichloride; In methanol; dichloromethane; water;
DOI:10.1246/bcsj.64.576