(4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

Base Information

Chemical Name:(4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine
CAS No.:230623-61-7
Molecular Formula:C₃₃H₄₇NO₂Si
Molecular Weight:517.827
Hs Code.:

(4-{2-[3-(<i>tert</i>-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

Synonyms:(4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

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Chemical Property of (4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

Chemical Property:

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Technology Process of (4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

There total 2 articles about (4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 3-(2-{4-[(4-butyl-phenyl)-phenyl-amino]-phenyl}-ethoxy)-propan-1-ol

: 230623-61-7
(4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

Guidance literature:: With 1H-imidazole; In dichloromethane; N,N-dimethyl-formamide; for 1.5h; Ambient temperature;
DOI:10.1021/jo981707v

Reference yield:

: [4-(2-allyloxy-ethyl)-phenyl]-(4-butyl-phenyl)-phenyl-amine

: 230623-61-7
(4-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-ethyl}-phenyl)-(4-butyl-phenyl)-phenyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 9-BBN, 2.) aq. NaOH, aq. H₂O₂ / 1.) THF, room temperature, 24 h, 2.) 50 deg C, 2 h

2: 87 percent / imidazole / dimethylformamide; CH₂Cl₂ / 1.5 h / Ambient temperature

With 1H-imidazole; sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo981707v