toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester
CAS No.:1369205-81-1
Molecular Formula:C₂₁H₂₉NO₄S
Molecular Weight:391.532
Hs Code.:

Synonyms:toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

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Chemical Property of toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

Chemical Property:

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Technology Process of toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

There total 5 articles about toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369205-94-6
toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

: 2386-64-3
ethylmagnesium chloride

: 1369205-81-1
toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

Guidance literature:: In tetrahydrofuran; at 25 - 30 ℃; for 3h;

Reference yield:

: 13103-80-5
1-(3-hydroxyphenyl)propan-1-one

: 1369205-81-1
toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water; isopropyl alcohol / 16 h / Reflux

2: potassium carbonate / dichloromethane / 1 h / 30 - 35 °C

3: tetrahydrofuran / 3 h / 25 - 30 °C

With hydrogenchloride; potassium carbonate; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1369205-81-1
toluene-4-sulfonic acid 3-(3-dimethylamino-1-ethyl-1-hydroxy-2-methylpropyl)phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dichloromethane / 1 h / 0 - 35 °C

2: hydrogenchloride / water; isopropyl alcohol / 12 h / Reflux

3: tetrahydrofuran / 3 h / 25 - 30 °C

With hydrogenchloride; potassium carbonate; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;