toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester
CAS No.:1369205-94-6
Molecular Formula:C₁₉H₂₃NO₄S
Molecular Weight:361.462
Hs Code.:

Synonyms:toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

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Chemical Property of toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

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Technology Process of toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

There total 4 articles about toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1343471-61-3
rac-3-(dimethylamino)-1-(3-hydroxyphenyl)-2-methylpropan-1-one

: 98-59-9
p-toluenesulfonyl chloride

: 1369205-94-6
toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Guidance literature:: With potassium carbonate; In dichloromethane; at 30 - 35 ℃; for 1h;

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1369205-80-0
toluene-4-sulfonic acid 3-propionylphenyl ester

: 506-59-2
N,N-dimethylammonium chloride

: 1369205-94-6
toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Guidance literature:: With hydrogenchloride; In water; isopropyl alcohol; for 12h; Reflux;

Reference yield:

: 13103-80-5
1-(3-hydroxyphenyl)propan-1-one

: 1369205-94-6
toluene-4-sulfonic acid 3-(3-dimethylamino-2-methylpropionyl)phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / isopropyl alcohol; water / 16 h / Reflux

2: potassium carbonate / dichloromethane / 1 h / 30 - 35 °C

With hydrogenchloride; potassium carbonate; In dichloromethane; water; isopropyl alcohol;