N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

Base Information

Chemical Name:N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride
CAS No.:1206789-18-5
Molecular Formula:C₂₃H₂₈N₄O₂*ClH
Molecular Weight:428.962
Hs Code.:

Synonyms:N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

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Chemical Property of N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

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Technology Process of N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

There total 5 articles about N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 108038-52-4
3H-benzo[d]imidazole-5-carbohydrazide

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 1206789-18-5
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

Guidance literature:: 3H-benzo[d]imidazole-5-carbohydrazide; 3,5-di-tert-butyl-2-hydroxybenzaldehyde; In ethanethiol; for 6h; Reflux;

With hydrogenchloride; In ethanol; at 20 ℃; for 0.5h; pH=1 - 2;

Reference yield:

: 1206789-73-2
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

: 1206789-18-5
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 20 ℃; for 0.5h; pH=1 - 2;

Reference yield:

: 619-05-6
3,4-diaminobenzoic acid

: 1206789-18-5
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 3 h / Reflux

2.1: 7 h / Reflux

2.2: pH 7

3.1: hydrazine hydrate / ethanol / 4 h / Reflux

4.1: ethanethiol / 6 h / Reflux

4.2: 0.5 h / 20 °C / pH 1 - 2

With hydrazine hydrate; sulfuric acid; In ethanol; ethanethiol;