N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

Base Information

Chemical Name:N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide
CAS No.:1206789-73-2
Molecular Formula:C₂₃H₂₈N₄O₂
Molecular Weight:392.501
Hs Code.:

Synonyms:N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

Chemical Property:

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Technology Process of N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

There total 4 articles about N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108038-52-4
3H-benzo[d]imidazole-5-carbohydrazide

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 1206789-73-2
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

Guidance literature:: In ethanol; for 6h; Reflux;

Reference yield:

: 619-05-6
3,4-diaminobenzoic acid

: 1206789-73-2
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 3 h / Reflux

1.2: pH 7 / Cooling with ice

2.1: pH 7 / Reflux

2.2: pH 7 / Cooling with ice

3.1: hydrazine hydrate / ethanol / 4 h / Reflux

4.1: ethanol / 6 h / Reflux

With sulfuric acid; hydrazine hydrate; In ethanol;

Reference yield:

: 37466-90-3
ethyl 3,4-diaminobenzoate

: 1206789-73-2
N'-[(2-hydroxy-3,5-di-tert-butyl)phenylmethylene]-1H-benzo[d]imidazole-6-formhydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pH 7 / Reflux

1.2: pH 7 / Cooling with ice

2.1: hydrazine hydrate / ethanol / 4 h / Reflux

3.1: ethanol / 6 h / Reflux

With hydrazine hydrate; In ethanol;