1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

Base Information

Chemical Name:1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine
CAS No.:1048993-80-1
Molecular Formula:C₁₉H₁₆ClN₃O
Molecular Weight:337.809
Hs Code.:

Synonyms:1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

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Chemical Property of 1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

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Technology Process of 1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

There total 2 articles about 1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1048990-90-4
1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazole-3-carboxylic acid

: 1048993-80-1
1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

Guidance literature:: 1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazole-3-carboxylic acid; With thionyl chloride; In dichloromethane; at 50 ℃; for 1.5h;

With sodium azide; In water; acetone;

With hydrogenchloride; water; In dichloromethane; at 100 - 110 ℃; for 4h;

Reference yield:

: 1048993-75-4
2-(trimethylsilyl)ethyl {1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-yl}carbamate

: 1048993-80-1
1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 23h; Product distribution / selectivity;

Reference yield:

: 1048993-80-1
1-[(5-chloro-2-phenyl-benzofuran-7-yl)methyl]-5-methyl-1H-pyrazol-3-amine

: 163438-09-3
(R)-1-Boc-nipecotic acid

: 1048994-11-1
1,1-dimethylethyl (3R)-3-(((1-((5-chloro-2-phenyl-benzofuran-7-yl)methyl)-5-methyl-1H-pyrazol-3-yl)amino)carbonyl)-1-piperidinecarboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 18h;