(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

Base Information

Chemical Name:(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester
CAS No.:1028300-26-6
Molecular Formula:C₃₂H₃₄N₂O₉
Molecular Weight:590.63
Hs Code.:

Synonyms:(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

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Chemical Property of (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

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Technology Process of (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

There total 1 articles about (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 157886-31-2
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid

: 70-11-1
α-bromoacetophenone

: 1028300-26-6
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

: 218443-23-3
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

Guidance literature:: In 1,4-dioxane; water; for 96h; Yield given;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4

Reference yield: 100.0%

: 1028300-26-6
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

: (S,S)-7-amino-2-<<(benzyloxy)carbonyl>amino>octanedioic acid 1-(2-oxo-2-phenylethyl) ester 7-(N-carboxyanhydride)

Guidance literature:: With Dichloromethyl methyl ether; at 20 - 60 ℃; for 2.5h;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4

Reference yield:

: 1028300-26-6
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid 2-oxo-2-phenylethyl ester

: (S,S)-2-amino-7-<<(benzyloxy)carbonyl>amino>octanedioic acid 8-(2-oxo-2-phenylethyl) ester acetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₃OCHCl₂ / 2.5 h / 20 - 60 °C

2: 100 percent / H₂O / 12 h / Ambient temperature

With Dichloromethyl methyl ether; water;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4