N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

Base Information

Chemical Name:N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide
CAS No.:1422975-95-8
Molecular Formula:C₄₇H₃₉N₃O₆
Molecular Weight:741.843
Hs Code.:

Synonyms:N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

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Chemical Property of N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

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Technology Process of N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

There total 4 articles about N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1312002-41-7
4,6-dimethoxy-2,3-diphenyl-7-trichloroacetylindole

: 2-amino-1-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-ethanone hydrochloride

: 1422975-95-8
N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

Guidance literature:: With triethylamine; In acetonitrile; Reflux;
DOI:10.1016/j.tet.2012.12.084

Reference yield:

: 100997-46-4
4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carbaldehyde

: 1422975-95-8
N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / Reflux

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 20 °C

3: hydrogen; palladium 10% on activated carbon; acetic acid / ethyl acetate / 20 h / 20 °C

4: triethylamine / acetonitrile / Reflux

With palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tet.2012.12.084

Reference yield:

: 1422975-80-1
2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-(trimethylsilyloxy)acetonitrile

: 1422975-95-8
N-(2-(4,6-dimethoxy-2,3-diphenyl-1H-indol-7-yl)-2-oxoethyl)-4,6-dimethoxy-2,3-diphenyl-1H-indole-7-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 20 °C

2: hydrogen; palladium 10% on activated carbon; acetic acid / ethyl acetate / 20 h / 20 °C

3: triethylamine / acetonitrile / Reflux

With palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; ethyl acetate; acetonitrile;
DOI:10.1016/j.tet.2012.12.084