(7-AMINO-2,3-DIHYDRO-BENZO[1,4]DIOXIN-6-YL)-(4-CHLORO-PHENYL)-METHANONE

Base Information

• Chemical Name: (7-AMINO-2,3-DIHYDRO-BENZO[1,4]DIOXIN-6-YL)-(4-CHLORO-PHENYL)-METHANONE
• CAS No.: 696628-26-9
• Molecular Formula: C₁₅H₁₂ClNO₃
• Molecular Weight: 289.718
• Mol file: 696628-26-9.mol

Synonyms:6-amino-7-(4-chlorobenzoyl)-1,4-benzodioxane

Chemical Property of (7-AMINO-2,3-DIHYDRO-BENZO[1,4]DIOXIN-6-YL)-(4-CHLORO-PHENYL)-METHANONE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

(7-Amino-2,3-dihydrobenzo[b][1,4]dioxin-6-yl)(4-chlorophenyl)methanone 97% ^*data from reagent suppliers

Safty Information:

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Technology Process of (7-AMINO-2,3-DIHYDRO-BENZO[1,4]DIOXIN-6-YL)-(4-CHLORO-PHENYL)-METHANONE

There total 1 articles about (7-AMINO-2,3-DIHYDRO-BENZO[1,4]DIOXIN-6-YL)-(4-CHLORO-PHENYL)-METHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C15H10ClNO5 (696628-19-0) → 6-amino-7-(4-chlorobenzoyl)-1,4-benzodioxane (696628-26-9)

Guidance literature:

C₁₅H₁₀ClNO₅; With iron; In benzene; at 75 ℃; for 0.5h;

With water; In benzene; at 80 ℃;

DOI:10.1007/s10593-010-0409-1

Reference yield: 83.0%

6-amino-7-(4-chlorobenzoyl)-1,4-benzodioxane (696628-26-9) + n-valeryl chloride (638-29-9) → C20H20ClNO4 (936079-40-2)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 0.5h;

DOI:10.1007/s10593-011-0881-2

Reference yield: 52.0%

6-amino-7-(4-chlorobenzoyl)-1,4-benzodioxane (696628-26-9) + Nitrosobenzene (586-96-9) → C21H15ClN2O3 (1018048-49-1)

Guidance literature:

With acetic acid; at 20 ℃; for 8h;

DOI:10.1007/s10593-010-0409-1

upstream raw materials:

C₁₅H₁₀ClNO₅

Downstream raw materials:

C₂₁H₁₅ClN₂O₃

C₂₀H₂₀ClNO₄

C₂₀H₁₈ClNO₃

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