N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N₁-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide

Base Information

• Chemical Name: N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N₁-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide
• CAS No.: 1224157-68-9
• Molecular Formula: C₉₀H₁₃₄N₁₀O₂₂
• Molecular Weight: 1708.11

Synonyms:N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N₁-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide

Chemical Property of N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N₁-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide

Chemical Property:

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Technology Process of N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N₁-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide

There total 1 articles about N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N₁-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

N-tert-butoxycarbonyl-3-aminopropanol (58885-58-8) + N,N'-bis-(N1,N4,N9-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxydiimide (1224157-57-6) → N,N'-bis-(N1,N4,N9-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-bis-(N1-tert-butoxycarbonyl-3-hydroxypropyl)perylene-3,4:9,10-tetracarboxydiimide (1224157-68-9)

Guidance literature:

N-tert-butoxycarbonyl-3-aminopropanol; With sodium hydride; at 20 ℃; for 0.333333h;

N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxydiimide; In 1,4-dioxane; at 90 ℃; for 19h;

DOI:10.1039/b917287d

upstream raw materials:

N-tert-butoxycarbonyl-3-aminopropanol

N,N'-bis-(N₁,N₄,N₉-tri-tert-butoxycarbonyl-12-amino-4,9-diazadodecyl)-1,7-dibromoperylene-3,4:9,10-tetracarboxydiimide

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