tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

Base Information

Chemical Name:tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate
CAS No.:350487-05-7
Molecular Formula:C₂₆H₃₄N₆O₆
Molecular Weight:526.593
Hs Code.:

tert-butyl 4-(N<sup>6</sup>-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

Synonyms:tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

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Chemical Property of tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

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Technology Process of tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

There total 2 articles about tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 82919-04-8
(N⁶-benzyloxycarbonyl)adenine

: 163210-89-7
tert-butyl (S)-2-[(tert-butoxycarbonyl)amino]-4-bromobutanoate

: 350487-05-7
tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1016/S0968-0896(00)00324-2

Reference yield:

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 350487-05-7
tert-butyl 4-(N⁶-benzyloxycarbonyladenin-9-yl)-2S-butoxycarbonylaminobutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / CBrCl₃; 2-mercaptopyridine N-oxide; DCC / DMAP / tetrahydrofuran / 4 h / 0 - 20 °C / Irradiation

2: 47 percent / K₂CO₃; Cs₂CO₃; TBAI / dimethylformamide / 50 °C

With Bromotrichloromethane; tetra-(n-butyl)ammonium iodide; potassium carbonate; caesium carbonate; dicyclohexyl-carbodiimide; 2-mercaptopyridine N-oxide; dmap; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(00)00324-2