(2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

Base Information

Chemical Name:(2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone
CAS No.:223545-30-0
Molecular Formula:C₁₈H₂₃NO₃
Molecular Weight:301.386
Hs Code.:

Synonyms:(2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

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Technology Process of (2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

There total 7 articles about (2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 223545-28-6
(R)-2-((R)-2-Methyl-pent-4-enyl)-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid phenyl ester

: 223545-30-0
(2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

Guidance literature:: With acetic acid; zinc; for 17h; Inert atmosphere;
DOI:10.1021/jo1019688

Reference yield:

: 223545-26-4
(R)-2-((R)-2-Methyl-pent-4-enyl)-2,3-dihydro-1H-pyridin-4-one

: 223545-30-0
(2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / n-BuLi

2: 86 percent / L-selectride, BF₃*OEt₂ / tetrahydrofuran / -23 °C

With n-butyllithium; boron trifluoride diethyl etherate; L-Selectride; In tetrahydrofuran;
DOI:10.1021/jo990192k

Reference yield:

: 126378-42-5
4-methoxy-3-(trisopropylsilyl)pyridine

: 223545-30-0
(2R)-2-[(R)-2-methyl-4-pentenyl]-1-(phenoxycarbonyl)-2,3,5,6-tetrahydro-4-pyridone

Guidance literature:: Multi-step reaction with 5 steps

2: 2.) H₃O⁺

3: 1.) NaOMe, 2.) 10 percent HCl / 1.) MeOH

4: 100 percent / n-BuLi

5: 86 percent / L-selectride, BF₃*OEt₂ / tetrahydrofuran / -23 °C

With hydrogenchloride; n-butyllithium; boron trifluoride diethyl etherate; oxonium; sodium methylate; L-Selectride; In tetrahydrofuran;
DOI:10.1021/jo990192k