1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

Base Information

Chemical Name:1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone
CAS No.:107343-20-4
Molecular Formula:C₂₄H₂₉NO₅
Molecular Weight:411.498
Hs Code.:

Synonyms:1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

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Chemical Property of 1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

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Technology Process of 1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

There total 5 articles about 1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 90158-33-1
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

: 107343-20-4
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

: 89680-93-3
5-acetyl-1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-2-piperidone

Guidance literature:: With Hg(OAc)2*EDTA; In acetic acid; Heating;
DOI:10.1248/cpb.33.5316

Reference yield:

: 55676-25-0
3-(2-methyl-[1,3]dioxolan-2-yl)-pyridine

: 107343-20-4
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / benzene / 5 h / Ambient temperature

2: 1.) H₂; 2.) NaBH₄ / 1.) Adams catalyst / 1.) ethanol/water, 18 h, room temperature; 2.) ethanol/water, room temperature

3: 98 percent / 1N HCl / H₂O / 2 h / 40 °C

4: 10 percent / Hg(OAc)2-EDTA / aq. acetic acid / Heating

With hydrogenchloride; sodium tetrahydroborate; Hg(OAc)2*EDTA; hydrogen; platinum(IV) oxide; In water; acetic acid; benzene;
DOI:10.1248/cpb.33.5316

Reference yield:

: 56774-66-4
2-(benzyloxy)-3,4-dimethoxyphenacyl bromide

: 107343-20-4
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / benzene / 5 h / Ambient temperature

2: 1.) H₂; 2.) NaBH₄ / 1.) Adams catalyst / 1.) ethanol/water, 18 h, room temperature; 2.) ethanol/water, room temperature

3: 98 percent / 1N HCl / H₂O / 2 h / 40 °C

4: 10 percent / Hg(OAc)2-EDTA / aq. acetic acid / Heating

With hydrogenchloride; sodium tetrahydroborate; Hg(OAc)2*EDTA; hydrogen; platinum(IV) oxide; In water; acetic acid; benzene;
DOI:10.1248/cpb.33.5316