2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester

Base Information

• Chemical Name: 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester
• CAS No.: 824955-28-4
• Molecular Formula: C₂₁H₃₀N₂O₄S
• Molecular Weight: 406.546
• Mol file: 824955-28-4.mol

Synonyms:2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester

Chemical Property of 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester

There total 2 articles about 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-Cysteine (52-90-4) + (E,E)-8-O-(2-N-methyl-aminobenzoyl)-3,7-dimethyl-2,6-octadiene-1-chloride (330641-20-8) → 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester (824955-28-4)

Guidance literature:

With ammonia; In methanol; at 0 - 20 ℃; for 4h;

DOI:10.1002/anie.200461150

Reference yield:

l-cysteine hydrochloride (52-89-1) + (E,E)-8-O-(2-N-methyl-aminobenzoyl)-3,7-dimethyl-2,6-octadiene-1-chloride (330641-20-8) → 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester (824955-28-4)

Guidance literature:

With ammonia; In methanol; at 0 - 20 ℃; for 4h;

DOI:10.1002/chem.200500476

Reference yield:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) + 2-Methylamino-benzoic acid (2E,6E)-8-((R)-2-amino-2-carboxy-ethylsulfanyl)-2,6-dimethyl-octa-2,6-dienyl ester (824955-28-4) → 2-Methylamino-benzoic acid (2E,6E)-8-[(R)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)-ethylsulfanyl]-2,6-dimethyl-octa-2,6-dienyl ester

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1002/anie.200461150

upstream raw materials:

L-Cysteine

(E,E)-8-O-(2-N-methyl-aminobenzoyl)-3,7-dimethyl-2,6-octadiene-1-chloride

l-cysteine hydrochloride