N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Base Information

Chemical Name:N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide
CAS No.:1221148-08-8
Molecular Formula:C₃₇H₄₆N₂O₁₂S₂
Molecular Weight:774.91
Hs Code.:

Synonyms:N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

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Technology Process of N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

There total 1 articles about N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1062080-87-8
N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: 2258-42-6
formyl acetic anhydride

: 1221148-08-8
N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Guidance literature:: With pyridine; dmap; at -20 ℃;
DOI:10.3762/bjoc.6.23

Reference yield: 85.0%

: 1221148-08-8
N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: 1221148-10-2
C₃₃H₃₄N₂O₁₂

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.3762/bjoc.6.23