N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Base Information

• Chemical Name: N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide
• CAS No.: 1062080-87-8
• Molecular Formula: C₃₅H₄₆N₂O₁₀S₂
• Molecular Weight: 718.89

Synonyms:N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Chemical Property of N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

There total 1 articles about N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl-2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside (501088-64-8) + 2,2-Dimethylmalonyl chloride (5659-93-8) → N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide (1062080-87-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1055/S-2008-1078419

Reference yield: 98.0%

N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide (1062080-87-8) + formyl acetic anhydride (2258-42-6) → N,N'-bis(ethyl 3-O-formyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide (1221148-08-8)

Guidance literature:

With pyridine; dmap; at -20 ℃;

DOI:10.3762/bjoc.6.23

Reference yield: 97.0%

N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide (1062080-87-8) + acetic anhydride (108-24-7) → N,N'-bis(ethyl-3-O-acetyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide (1062080-91-4)

Guidance literature:

With pyridine; at 20 ℃; for 16h;

DOI:10.1055/S-2008-1078419

upstream raw materials:

ethyl-2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

2,2-Dimethylmalonyl chloride

Downstream raw materials:

N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

N,N'-bis(ethyl-3-O-acetyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

N,N'-bis(ethyl-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-methyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1062080-87-8 N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send