1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

Base Information

Chemical Name:1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide
CAS No.:1355255-05-8
Molecular Formula:C₂₃H₂₆N₃O₂*I
Molecular Weight:503.383
Hs Code.:

Synonyms:1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

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Chemical Property of 1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

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Technology Process of 1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

There total 4 articles about 1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1355255-03-6
2-(4-methylphenylamino)-3-(4-methylpiperazin-1-yl)-1,4-dihydronaphthalene-1,4-dione

: 74-88-4
methyl iodide

: 1355255-05-8
1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 48h; Darkness;
DOI:10.1134/S1070428011120086

Reference yield:

: 109-01-3
1-methyl-piperazine

: 1355255-05-8
1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3.5 h / 20 °C

2: potassium hydroxide / 1,4-dioxane; methanol / 12 h

3: triethylamine / ethanol / 48 h / 20 °C / Darkness

With triethylamine; potassium hydroxide; In 1,4-dioxane; methanol; ethanol;
DOI:10.1134/S1070428011120086

Reference yield:

: 84348-94-7
NSC₁₂₉₀₇₇

: 1355255-05-8
1,1-dimethyl-4-[3-(4-methylphenylamino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl]piperazinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3.5 h / 20 °C

2: potassium hydroxide / 1,4-dioxane; methanol / 12 h

3: triethylamine / ethanol / 48 h / 20 °C / Darkness

With triethylamine; potassium hydroxide; In 1,4-dioxane; methanol; ethanol;
DOI:10.1134/S1070428011120086