4-tert-butyl-N-(tritylsulfanyl)cyclohexanimine

Base Information

Chemical Name:4-tert-butyl-N-(tritylsulfanyl)cyclohexanimine
CAS No.:86864-29-1
Molecular Formula:C29H33 N S
Molecular Weight:427.644
Hs Code.:

Synonyms:Benzenemethanesulfenamide,N-[4-(1,1-dimethylethyl)cyclohexylidene]-a,a-diphenyl- (9CI); NSC 378992

Suppliers and Price of 4-tert-butyl-N-(tritylsulfanyl)cyclohexanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-butyl-N-(tritylsulfanyl)cyclohexanimine

Chemical Property:

Vapor Pressure:3.67E-11mmHg at 25°C
Boiling Point:539.5°C at 760 mmHg
Flash Point:280.1°C
Density:1.03g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-tert-butyl-N-(tritylsulfanyl)cyclohexanimine

There total 3 articles about 4-tert-butyl-N-(tritylsulfanyl)cyclohexanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 38499-08-0
Triphenylmethanesulfenamide

: 98-53-3
4-tercbutyl-cyclohexanone

: 86864-29-1
C₂₉H₃₃NS

Guidance literature:: With pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo00168a031

Reference yield:

: 3695-77-0
triphenylmethanethiol

: 86864-29-1
C₂₉H₃₃NS

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Sulfuryl chloride / toluene; diethyl ether / 2 h / 0 °C

2: 78 percent / 29 percent NH₄OH/H₂O / CH₂Cl₂ / 0 °C

3: 99 percent / Pyridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO₄ / CH₂Cl₂ / 2 h / Ambient temperature

With ammonium hydroxide; sulfuryl dichloride; water; pyridinium p-toluenesulfonate; magnesium sulfate; In diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00168a031

Reference yield:

: 24165-03-5
tritylsulfenyl chloride

: 86864-29-1
C₂₉H₃₃NS

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 29 percent NH₄OH/H₂O / CH₂Cl₂ / 0 °C

2: 99 percent / Pyridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO₄ / CH₂Cl₂ / 2 h / Ambient temperature

With ammonium hydroxide; water; pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane;
DOI:10.1021/jo00168a031