[1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester

Base Information

• Chemical Name: [1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester
• CAS No.: 94903-80-7
• Molecular Formula: C₁₅H₂₂O₄
• Molecular Weight: 266.337

Synonyms:[1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester

Chemical Property of [1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester

Chemical Property:

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Technology Process of [1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester

There total 1 articles about [1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ pyridine (110-86-1) + [1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester (94903-80-7)

Guidance literature:

Reference yield: 83.0%

[1S-[1α,2α(5Z)3α,4α]]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester (94903-80-7) + 4-phenyl-semicarbazide (537-47-3) → methyl <1S-<1α,2α(Z),3α,4α>>-7-<3-<<2-<(phenylamino)carbonyl>hydrazono>methyl>-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoate (128781-28-2,128821-63-6)

Guidance literature:

In methanol; for 6h; Ambient temperature;

DOI:10.1021/jm00171a021

Reference yield:

1-Ethyl-1-benzoyl hydrazine (5501-18-8) + [1β,2α(5Z),3β,4β]-7-[3-Formyl-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester (70120-35-3,71884-49-6,74868-26-1,74868-27-2,89395-86-8,89395-87-9,94903-80-7,96444-22-3,98717-73-8,104320-49-2,104596-33-0,121423-88-9,121423-94-7) → [1β,2α(5Z),3β,4β]-7-[3-[(Ethylbenzoylhydrazono)methyl]-7-oxabicyclo[2.2.1]hept-2-yl]-5-heptenoic acid, methyl ester

Guidance literature:

In ethanol;

Downstream raw materials:

(Z)-7-[(1S,2R,3S,4R)-3-((E)-3-Cyclohexyl-3-oxo-propenyl)-7-oxa-bicyclo[2.2.1]hept-2-yl]-hept-5-enoic acid methyl ester

methyl <1S-<1α,2α(Z),3α(E),4α>>-7-<3-<3-oxo-4-<4-(tert-butyldimethylsiloxy)phenyl>-1-pentenyl>-7-oxabicyclo<2.2.1>hept-2-yl>-5-heptenoate

(Z)-7-[(1S,2R,3S,4R)-3-((E)-(R)-3-Oxo-4-phenyl-pent-1-enyl)-7-oxa-bicyclo[2.2.1]hept-2-yl]-hept-5-enoic acid methyl ester

(Z)-7-[(1S,2R,3S,4R)-3-((E)-(S)-3-Oxo-4-phenyl-pent-1-enyl)-7-oxa-bicyclo[2.2.1]hept-2-yl]-hept-5-enoic acid methyl ester

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