2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

Base Information

Chemical Name:2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside
CAS No.:1001082-66-1
Molecular Formula:C₃₀H₃₂O₉
Molecular Weight:536.579
Hs Code.:

Synonyms:2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

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Chemical Property of 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

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Technology Process of 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

There total 1 articles about 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1001082-65-0
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

: 123-76-2
levulinic acid

: 1001082-66-1
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 2.33333h;
DOI:10.1021/jo701531x

Reference yield: 95.0%

: 1001082-66-1
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

: 1001082-67-2
2'-(allyloxycarbonyl)benzyl 6-O-benzyl-2-O-levulinyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃; for 4h;
DOI:10.1021/jo701531x