1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

Base Information

Chemical Name:1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole
CAS No.:1146690-03-0
Molecular Formula:C₁₈H₁₂F₁₅N₃OS
Molecular Weight:603.355
Hs Code.:

Synonyms:1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

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Chemical Property of 1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

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Technology Process of 1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

There total 8 articles about 1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₁₄F₁₅N₃O₂S

: 1146690-03-0
1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

Guidance literature:: With hydrogenchloride; water; In ethanol; for 1h; Reflux;

Reference yield:

: 2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenylhydrazine

: 1146690-03-0
1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 0.08 h / 20 °C

1.2: 3 h / Reflux

1.3: pH 7

2.1: toluene / 12 h / Reflux

3.1: ammonia; water / ethanol / 0.5 h / 20 °C

4.1: pyridine / dichloromethane / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / cooling with ice

5.2: 1 h / 20 °C

6.1: hydrogenchloride; water / ethanol / 1 h / Reflux

With pyridine; hydrogenchloride; ammonia; water; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 638-79-9
undecafluoro-1-iodopentane

: 1146690-03-0
1-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}-5-methylamino-3-(1,1,2,2,3,3,4,4,5,5,5-undecafluoropentyloxy)pyrazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: dihydrogen peroxide; trifluoroacetic acid; trifluoroacetic anhydride / -10 - 20 °C

1.2: 20 °C / cooling with ice

2.1: pyridine / dichloromethane / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / cooling with ice

3.2: 1 h / 20 °C

4.1: hydrogenchloride; water / ethanol / 1 h / Reflux

With pyridine; hydrogenchloride; water; dihydrogen peroxide; sodium hydride; trifluoroacetic acid; trifluoroacetic anhydride; In ethanol; dichloromethane; N,N-dimethyl-formamide;