2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

Base Information

Chemical Name:2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate
CAS No.:150461-50-0
Molecular Formula:C₃₃H₃₁ClN₂O₄S₂
Molecular Weight:619.205
Hs Code.:

Synonyms:2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

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Chemical Property of 2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

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Technology Process of 2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

There total 11 articles about 2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: 150461-49-7
2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol

: 150461-50-0
2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jm00071a008

Reference yield:

: 3256-88-0
5-phenyl-2-picoline

: 150461-50-0
2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / N-chlorosuccinimide, benzoyl peroxide / CCl₄ / 5 h / Heating; Irradiation

2: NaH / dimethylformamide / 1 h

3: 95 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

4: 100 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With N-chloro-succinimide; lithium aluminium tetrahydride; Perbenzoic acid; sodium hydride; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00071a008

Reference yield:

: 146775-28-2
2-chloromethyl-5-phenylpyridine

: 150461-50-0
2-<1-(4-chlorobenzyl)-4-methyl-6-<(5-phenylpyridin-2-yl)methoxy>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>ethanol methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 1 h

2: 95 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

3: 100 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00071a008