(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

Base Information

Chemical Name:(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester
CAS No.:201472-18-6
Molecular Formula:C₂₆H₃₈O₅Si
Molecular Weight:458.67
Hs Code.:

Synonyms:(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

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Chemical Property of (R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

Chemical Property:

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Technology Process of (R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

There total 3 articles about (R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128075-94-5
(R)-5-{[(tert-butyldiphenylsilyl)oxy]methyl}dihydrofuran-2(3H)-one

: 201472-18-6
(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / DIBAL-H / toluene / 1 h / -78 °C

2: 92 percent / PhCO₂H / CH₂Cl₂ / 12 h / Ambient temperature

3: 100 percent / H₂ / Pd/C / ethyl acetate / 2 h / 760 Torr / Ambient temperature

4: 695.0 mg / DIPEA / CH₂Cl₂ / 4 h / 0 - 20 °C

With hydrogen; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; benzoic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate; toluene;
DOI:10.1021/jo9713621

Reference yield:

: 201472-31-3
(E)-(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-hydroxy-hept-2-enoic acid methyl ester

: 201472-18-6
(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethyl acetate / 2 h / 760 Torr / Ambient temperature

2: 695.0 mg / DIPEA / CH₂Cl₂ / 4 h / 0 - 20 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jo9713621

Reference yield:

: 201472-30-2
(R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-tetrahydro-furan-2-ol

: 201472-18-6
(R)-7-(tert-Butyl-diphenyl-silanyloxy)-6-methoxymethoxy-heptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / PhCO₂H / CH₂Cl₂ / 12 h / Ambient temperature

2: 100 percent / H₂ / Pd/C / ethyl acetate / 2 h / 760 Torr / Ambient temperature

3: 695.0 mg / DIPEA / CH₂Cl₂ / 4 h / 0 - 20 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; benzoic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jo9713621