3-methyl-5-phenyl-4-pentenol

Base Information

Chemical Name:3-methyl-5-phenyl-4-pentenol
CAS No.:73408-01-2
Molecular Formula:C₁₂H₁₆O
Molecular Weight:176.258
Hs Code.:

Synonyms:3-methyl-5-phenyl-4-pentenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-5-phenyl-4-pentenol

Chemical Property:

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Technology Process of 3-methyl-5-phenyl-4-pentenol

There total 2 articles about 3-methyl-5-phenyl-4-pentenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 7796-71-6
3-methyl-4-pentenoic acid ethyl ester

: 73408-01-2
3-methyl-5-phenyl-4-pentenol

: 55066-48-3
3-methyl-5-phenylpentan-1-ol

Guidance literature:: styrene; 3-methyl-4-pentenoic acid ethyl ester; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 50 ℃; for 3h; Inert atmosphere;

With potassium tert-butylate; hydrogen; (2-aminoethyl)diphenylphosphane; In tetrahydrofuran; at 110 ℃; for 16h; under 37503.8 Torr; Reagent/catalyst; Temperature; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c7gc00192d

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 7796-71-6
3-methyl-4-pentenoic acid ethyl ester

: 73408-01-2
3-methyl-5-phenyl-4-pentenol

Guidance literature:: styrene; 3-methyl-4-pentenoic acid ethyl ester; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 50 ℃; for 3h; Inert atmosphere;

With potassium tert-butylate; hydrogen; (2-aminoethyl)diphenylphosphane; In tetrahydrofuran; at 90 ℃; for 16h; under 37503.8 Torr; Reagent/catalyst; Temperature; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c7gc00192d

Reference yield:

: 73408-01-2
3-methyl-5-phenyl-4-pentenol

: 149713-23-5,149713-24-6
2-phenyl-4-methyltetrahydrpyran

: 149713-23-5,149713-24-6
2-phenyl-4-methyltetrahydrpyran

Guidance literature:: With aluminium(III) triflate; In 1,2-dichloro-ethane; for 3h; regioselective reaction; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.200900841