Ethyl 3-methylpent-4-enoate

Base Information

Chemical Name:Ethyl 3-methylpent-4-enoate
CAS No.:7796-71-6
Molecular Formula:C8H14O2
Molecular Weight:142.198
Hs Code.:
DSSTox Substance ID:DTXSID90499722
Nikkaji Number:J3.267.977C

Synonyms:ethyl 3-methylpent-4-enoate;ethyl 3-methyl-4-pentenoate;7796-71-6;SCHEMBL9796702;DTXSID90499722;AUAKFHKYJDJBKI-UHFFFAOYSA-N;3-methyl-pent-4-enoic acid ethyl ester

Suppliers and Price of Ethyl 3-methylpent-4-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Ethyl 3-methylpent-4-enoate

Chemical Property:

PSA：26.30000
LogP:1.76170
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:142.099379685
Heavy Atom Count:10
Complexity:118

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC(C)C=C

Technology Process of Ethyl 3-methylpent-4-enoate

There total 2 articles about Ethyl 3-methylpent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 563-52-0,35729-37-4
2-chloro-3-butene

: 5764-82-9
bromo(2-ethoxy-2-oxoethyl)zinc

: 34495-74-4
Ethyl 4-hexenoate

: 7796-71-6
3-methyl-4-pentenoic acid ethyl ester

Guidance literature:: copper acetylacetonate; In diethyl ether; dimethyl sulfoxide; at 25 ℃; for 2h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)88012-0

Reference yield:

: 4894-61-5
trans-but-2-enyl chloride

: 5764-82-9
bromo(2-ethoxy-2-oxoethyl)zinc

: 34495-74-4
Ethyl 4-hexenoate

: 7796-71-6
3-methyl-4-pentenoic acid ethyl ester

Guidance literature:: copper acetylacetonate; In diethyl ether; dimethyl sulfoxide; at 25 ℃; for 2h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)88012-0

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 7796-71-6
3-methyl-4-pentenoic acid ethyl ester

: 73408-01-2
3-methyl-5-phenyl-4-pentenol

: 55066-48-3
3-methyl-5-phenylpentan-1-ol

Guidance literature:: styrene; 3-methyl-4-pentenoic acid ethyl ester; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 50 ℃; for 3h; Inert atmosphere;

With potassium tert-butylate; hydrogen; (2-aminoethyl)diphenylphosphane; In tetrahydrofuran; at 110 ℃; for 16h; under 37503.8 Torr; Reagent/catalyst; Temperature; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c7gc00192d