C₅₅H₆₀Br₂O₅S₄

Base Information

• Chemical Name: C₅₅H₆₀Br₂O₅S₄
• CAS No.: 872115-32-7
• Molecular Formula: C₅₅H₆₀Br₂O₅S₄
• Molecular Weight: 1089.15
• Mol file: 872115-32-7.mol

Synonyms:C₅₅H₆₀Br₂O₅S₄

Chemical Property of C₅₅H₆₀Br₂O₅S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₆₀Br₂O₅S₄

There total 7 articles about C₅₅H₆₀Br₂O₅S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

[3-allyloxy-5-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(3-allyloxy-5-hydroxymethyl-benzylsulfanylmethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzylsulfanylmethyl)-phenyl]-methanol (872115-29-2) → C55H60Br2O5S4 (872115-32-7)

Guidance literature:

With pyridine; phosphorus tribromide; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1246/bcsj.78.1773

Reference yield:

[5-(prop-2-en-1-yloxy)benzene-1,3-diyl]dimethanol (156204-47-6) → C55H60Br2O5S4 (872115-32-7)

Guidance literature:

Multi-step reaction with 6 steps

1: 28 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

2: 2.75 g / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

3: 74 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C

5: 877 mg / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

6: 66 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

With pyridine; sodium hydroxide; phosphorus tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1246/bcsj.78.1773

Reference yield:

1-allyloxy-3-bromomethyl-5-hydroxymethylbenzene (872115-27-0) → C55H60Br2O5S4 (872115-32-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 2.75 g / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

2: 74 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 20 °C

4: 877 mg / NaOH / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

5: 66 percent / phosphorus tribromide; pyridine / CH₂Cl₂ / 24 h / 20 °C

With pyridine; sodium hydroxide; phosphorus tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1246/bcsj.78.1773

upstream raw materials:

[3-allyloxy-5-(3-allyloxy-5-{3-allyloxy-5-[3-allyloxy-5-(3-allyloxy-5-hydroxymethyl-benzylsulfanylmethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzylsulfanylmethyl)-phenyl]-methanol

1-allyloxy-3-bromomethyl-5-hydroxymethylbenzene

[5-(prop-2-en-1-yloxy)benzene-1,3-diyl]dimethanol

1-allyloxy-3,5-bis(bromomethyl)benzene

Downstream raw materials:

C₇₇H₈₆O₉S₆