carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)

Base Information

Chemical Name:carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)
CAS No.:100836-31-5
Molecular Formula:C₃₉H₃₀Cl₃O₃P₂Rh
Molecular Weight:817.877
Hs Code.:

Synonyms:carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)

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Chemical Property of carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)

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Technology Process of carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)

There total 1 articles about carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 41509-48-2,34735-89-2,38566-83-5
Rh(CF₃COO)(CO)(PPh₃)2

: 76-03-9
trichloroacetic acid

: 100836-31-5
carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)

Guidance literature:: In benzene; Cl3CCOOH was added to Rh-complex in benzene, stirred at ambient temp. for 1.5 h under N2; the solvent was removed under reduced pressure, residue was treated with MeOH;

Reference yield: 57.0%

: 100836-31-5
carbonyl(trichloroacetato)bis(triphenylphosphine)rhodium(I)

: 76-03-9
trichloroacetic acid

: 15318-33-9,16353-77-8,13938-94-8
chlorocarbonylbis(triphenylphosphine)rhodium(I)

Guidance literature:: With triphenylphosphine; In acetone; Cl3CCOOH and PPh3 were added to a soln. of Rh-complex in acetone, mixt.was stirred at ambient temp. for 10 min under N2; evapd. to dryness under reduced pressure, crystd. from CH2Cl2-hexane;