C₃₂H₂₈N₆O₄

Base Information

Chemical Name:C₃₂H₂₈N₆O₄
CAS No.:1307853-76-4
Molecular Formula:C₃₂H₂₈N₆O₄
Molecular Weight:560.612
Hs Code.:

C<sub>32</sub>H<sub>28</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₃₂H₂₈N₆O₄

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Chemical Property of C₃₂H₂₈N₆O₄

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Technology Process of C₃₂H₂₈N₆O₄

There total 14 articles about C₃₂H₂₈N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1307853-73-1
C₃₃H₃₀N₆O₄

: 1307853-76-4
C₃₂H₂₈N₆O₄

Guidance literature:: C₃₃H₃₀N₆O₄; With sodium hydroxide; In methanol; at 90 ℃; for 2h;

With hydrogenchloride; In water;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1307853-76-4
C₃₂H₂₈N₆O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium carbonate; tetrabutylammomium bromide / chloroform; water / 2 h / 55 °C / Cooling with ice

1.2: 1 h

2.1: potassium carbonate; triphenylphosphine / dichloro(1,5-cyclooctadiene)ruthenium(II) polymer / 1-methyl-pyrrolidin-2-one / 2 h / 140 °C / Inert atmosphere

3.1: sodium methylate / methanol / 1.5 h / 20 °C

4.1: phosphorus tribromide / tetrahydrofuran / 5.5 h / 0 - 20 °C

5.1: potassium carbonate / acetonitrile / 6 h / Reflux; Inert atmosphere

6.1: hydrogenchloride / methanol / 3.22 h / 3 - 9 °C

7.1: tin(II) chloride dihdyrate / methanol / 2 h / Reflux

8.1: acetic acid / 1 h / 90 °C

9.1: sodium hydroxide / methanol / 2 h / 90 °C

With hydrogenchloride; tin(II) chloride dihdyrate; tetrabutylammomium bromide; sodium methylate; phosphorus tribromide; sodium carbonate; potassium carbonate; acetic acid; triphenylphosphine; sodium hydroxide; dichloro(1,5-cyclooctadiene)ruthenium(II) polymer; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; chloroform; water; acetonitrile;

Reference yield:

: 18039-42-4,3999-10-8
5-Phenyl-1H-tetrazole

: 1307853-76-4
C₃₂H₂₈N₆O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium carbonate; tetrabutylammomium bromide / chloroform; water / 2 h / 55 °C / Cooling with ice

1.2: 1 h

2.1: potassium carbonate; triphenylphosphine / dichloro(1,5-cyclooctadiene)ruthenium(II) polymer / 1-methyl-pyrrolidin-2-one / 2 h / 140 °C / Inert atmosphere

3.1: sodium methylate / methanol / 1.5 h / 20 °C

4.1: phosphorus tribromide / tetrahydrofuran / 5.5 h / 0 - 20 °C

5.1: potassium carbonate / acetonitrile / 6 h / Reflux; Inert atmosphere

6.1: hydrogenchloride / methanol / 3.22 h / 3 - 9 °C

7.1: tin(II) chloride dihdyrate / methanol / 2 h / Reflux

8.1: acetic acid / 1 h / 90 °C

9.1: sodium hydroxide / methanol / 2 h / 90 °C

With hydrogenchloride; tin(II) chloride dihdyrate; tetrabutylammomium bromide; sodium methylate; phosphorus tribromide; sodium carbonate; potassium carbonate; acetic acid; triphenylphosphine; sodium hydroxide; dichloro(1,5-cyclooctadiene)ruthenium(II) polymer; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; chloroform; water; acetonitrile;