N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

Base Information

Chemical Name:N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide
CAS No.:529509-36-2
Molecular Formula:C₁₁H₁₆ClN₃O₅S
Molecular Weight:337.784
Hs Code.:

Synonyms:N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

Suppliers and Price of N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

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Technology Process of N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

There total 1 articles about N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67843-74-7,24969-06-0,13403-37-7
(S)-epichlorohydrin

: 83019-91-4
N-(2-aminoethyl)-2-nitrobenzene-sulfonamide

: 529509-36-2
N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

Guidance literature:: With magnesium sulfate; In methanol;

Reference yield: 31.0%

: 529509-36-2
N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

: 529509-37-3
1-(2-Nitro-benzenesulfonyl)-(6S)-[1,4]diazepan-6-ol

Guidance literature:: With caesium carbonate; In acetonitrile; at 65 ℃; for 6.5h;
DOI:10.1016/j.bmcl.2007.02.050

Reference yield:

: 529509-36-2
N-[2-({2S}-3-chloro-2-hydroxy-propylamino)-ethyl]-2-nitro-benzenesulfonamide

: C₂₆H₂₇FN₈O

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / Cs₂CO₃ / acetonitrile / 6.5 h / 65 °C

2: 85 percent / Et(i-Pr)2N / acetonitrile / 17 h / 102 °C

3: 92 percent / PhSH; K₂CO₃ / dimethylformamide / 0.83 h / 20 °C

With potassium carbonate; caesium carbonate; thiophenol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2007.02.050