C₆H₆INS

Base Information

• Chemical Name: C₆H₆INS
• CAS No.: 1262983-59-4
• Molecular Formula: C₆H₆INS
• Molecular Weight: 251.091
• Mol file: 1262983-59-4.mol

Synonyms:C₆H₆INS

Chemical Property of C₆H₆INS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₆INS

There total 3 articles about C₆H₆INS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(4-iodoanilin-2-yl)disulfide (1352149-35-9) → C6H6INS (1262983-59-4)

Guidance literature:

With 1,4-dithio-D,L-threitol; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

DOI:10.1002/ejoc.201100818

Reference yield:

p-aminoiodobenzene (540-37-4) → C6H6INS (1262983-59-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: bromine; acetic acid / 0.5 h / 10 °C

1.2: 19 h / 10 °C

2.1: potassium hydroxide / water; ethylene glycol / 24 h / 140 °C

3.1: 1,4-dithio-D,L-threitol / N,N-dimethyl-formamide / 0.5 h / 20 °C

With 1,4-dithio-D,L-threitol; bromine; acetic acid; potassium hydroxide; In water; ethylene glycol; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201100818

Reference yield:

6-iodobenzo[d]thiazol-2-amine (16582-58-4) → C6H6INS (1262983-59-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / water; ethylene glycol / 24 h / 140 °C

2: 1,4-dithio-D,L-threitol / N,N-dimethyl-formamide / 0.5 h / 20 °C

With 1,4-dithio-D,L-threitol; potassium hydroxide; In water; ethylene glycol; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201100818

upstream raw materials:

6-iodobenzo[d]thiazol-2-amine

bis(4-iodoanilin-2-yl)disulfide

p-aminoiodobenzene

Downstream raw materials:

6-iodo-N-phenylbenzo[d]thiazol-2-amine

6-iodo-N-p-tolylbenzo[d]thiazol-2-amine

6-iodo-1,3-benzothiazole