bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride

Base Information

• Chemical Name: bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride
• CAS No.: 59930-50-6
• Molecular Formula: C₆₀H₆₆IMoN₂P₄*Cl
• Molecular Weight: 1197.39

Synonyms:bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride

Chemical Property of bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride

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Technology Process of bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride

There total 1 articles about bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum (59930-49-3) → bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido(2-)-N)molybdenum chloride (59930-50-6)

Guidance literature:

With hydrogenchloride; In benzene; anhyd. HCl bubbled through benzene soln. MoI(N2C8H17)(dppe)2 for 0.33 h; soln. filtered, filtrate reduced and heptane added slowly with stirringand mixt. allowed to stand for 1.5 h, crystals filtered off,washed withheptane and dried in vacuo; elem. anal.;

DOI:10.1021/ic50215a007

upstream raw materials:

bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

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