(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane

Base Information

• Chemical Name: (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane
• CAS No.: 170117-43-8
• Molecular Formula: C₅₃H₅₀N₂O₈
• Molecular Weight: 842.989

Synonyms:(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane

Chemical Property of (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane

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Technology Process of (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane

There total 1 articles about (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) + (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane (170117-42-7) → (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane (170117-43-8)

Guidance literature:

With sodium hydrogencarbonate; In 1,4-dioxane; water; Ambient temperature;

DOI:10.1021/jm00016a001

Reference yield:

2,4-dimethyl-thiazole-5-carboxylic acid (53137-27-2) + Fmoc-Val-OH (68858-20-8) + (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane (170117-43-8) → C40H52N6O6S2

Guidance literature:

Multistep reaction;

DOI:10.1021/jm00016a001

Reference yield:

2-amino-4-thiazoleacetic acid (29676-71-9) + Fmoc-Val-OH (68858-20-8) + (4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-<(fluorenylmethyloxycarbonyl)amino>-2''-phenylethyl>-1,3-dioxolane (170117-43-8) → (S)-2-[2-(2-Amino-thiazol-4-yl)-acetylamino]-N-((1S,2R,3R,4S)-4-{(S)-2-[2-(2-amino-thiazol-4-yl)-acetylamino]-3-methyl-butyrylamino}-1-benzyl-2,3-dihydroxy-5-phenyl-pentyl)-3-methyl-butyramide

Guidance literature:

Multistep reaction;

DOI:10.1021/jm00016a001

upstream raw materials:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

(4R,5R,1''S)-1-methyl-1-(3'-carboxypropyl)-4,5-bis<1''-amino-2''-phenylethyl>-1,3-dioxolane

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