chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾

Base Information

• Chemical Name: chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾
• CAS No.: 126289-62-1
• Molecular Formula: C₁₃H₁₉ClMoNO₅P
• Molecular Weight: 431.664
• Mol file: 126289-62-1.mol

Synonyms:chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾

Chemical Property of chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾

Chemical Property:

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Technology Process of chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾

There total 1 articles about chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

bis(diethylamino)-t-butylphosphine(pentacarbonyl)molybdenum(0) (126306-22-7) → chlorodiethylamino-t-butylphosphine(pentacarbonyl)molybdenum(0) (126289-62-1) + diethyl amine hydrochloride (660-68-4)

Guidance literature:

With hydrogenchloride; In pentane; Under stirring a strong stream of hydrogenhalogenide is bubbled for 20 min through the soln. of phosphine complex at room temp.(inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., chromy., elem. anal.;

DOI:10.1016/0022-328X(89)85002-8

upstream raw materials:

bis(diethylamino)-t-butylphosphine(pentacarbonyl)molybdenum⁽⁰⁾

Refernces